Dimethylamine, hydrochloride → HCID 3554384, 화합물

HRID 622807노트

반응식

HRID 622807 반응식
Cl.[CH3:2][NH:3][CH3:4].[CH3:5][O:6][C:7](=[O:17])[C:8]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=[CH:9]O.[Na]>O>[CH3:5][O:6][C:7](=[O:17])[C:8]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=[CH:9][N:3]([CH3:4])[CH3:2]

참가 물질

4

반응물 2

HCID 10473Dimethylamine, hydrochlorideHCID 70407058HCID 70407058, 화합물

생성물 1

HCID 3554384HCID 3554384, 화합물수율 72.2%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

97 weight-parts of dimethylamine hydrochloride are dissolved in 250 weight-parts of water, and 200 weight-parts of sodium 3-hydroxy-2-phenyl acrylic acid methyl ester are added. The mixture is stirred for 2 hours, and the organic phase is separated and distilled. 148 weight-parts of 3-dimethylamino-2-phenyl acrylic acid methyl ester are obtained, corresponding to a yield of 72.2% of the theory.

후처리

  1. additionare added
  2. customthe organic phase is separated
  3. distillationdistilled

출처 및 근거

ORD 기록
ord-42f29bb6a9ac4b9d87ac01e86138f738
출처 데이터셋
uspto-grants-1988_09
특허 번호
US04772711

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