Thiophenol → Diphenyl sulfide

HRID 623238

반응식

HRID 623238 반응식
[C:1]1([SH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>C1(C)C=CC=CC=1>[C:1]1([S:7][C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

참가 물질

3

반응물 1

HCID 7969Thiophenol

생성물 1

HCID 8766Diphenyl sulfide

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

A mixture of bis(dineophyl-orthotrifluoromethylphenyltin)oxide (6.0 g, 5.6 mmol) prepared in Example 6, thiophenol (1.2 g, 11.2 mmol) and toluene (40 g) was treated with the procedure described in Example 7. The product was recrystallized from n-hexane to obtain 5.2 g of dineophylorthotrifluoromethylphenyltin phenylsulfide as a white solid.

후처리

  1. additionwas treated with the procedure
  2. customThe product was recrystallized from n-hexane

출처 및 근거

ORD 기록
ord-7087eac787814b4481a45eda5fa3f06b
출처 데이터셋
uspto-grants-1988_09
특허 번호
US04774235

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