Hydrochloric Acid → HCID 67126605, 화합물
반응식
Cl[C:2]1[CH:7]=[CH:6][C:5]([S:8]([NH2:11])(=[O:10])=[O:9])=[CH:4][C:3]=1[N+:12]([O-:14])=[O:13].[NH2:15][CH2:16][C:17]1([NH2:23])[CH2:22][CH2:21][O:20][CH2:19][CH2:18]1.Cl.C(N(CC)CC)C>O1CCOCC1.O>[NH2:23][C:17]1([CH2:16][NH:15][C:2]2[CH:7]=[CH:6][C:5]([S:8]([NH2:11])(=[O:10])=[O:9])=[CH:4][C:3]=2[N+:12]([O-:14])=[O:13])[CH2:22][CH2:21][O:20][CH2:19][CH2:18]1참가 물질
7
반응 조건
- 온도
- 110 °C
실험 절차
A mixture of 4-chloro-3-nitrobenzenesulfonamide, 4-(aminomethyl)tetrahydro-2H-pyran-4-amine, hydrochloric acid and triethylamine in dioxane (10 mL) was heated at 110° C. overnight. After cooling, the mixture was diluted with water (10 mL), and filtered.
후처리
- temperatureAfter cooling
- filtrationfiltered
출처 및 근거
- ORD 기록
- ord-f8d23405ece94d8b8d6f5b564b708e93
- 출처 데이터셋
- uspto-grants-2016_04
- 특허 번호
- US09303025B2
반응 노트
불러오는 중…