Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methylcyclohexanone → HCID 178424364, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methylcyclohexanone | HCID 11419 | — |
| 반응물 | 1-Phenethylamine, (+)- | HCID 643189 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | HCID 178424364 | HCID 178424364 | 84% |
반응 단계
A stirred solution of 2-methylcyclohexanone (5 g, 44.64 mmol) and (R)-1-phenylethanamine (5.4 g, 44.64 mmol) in toluene (50 mL) was maintained at 140-145° C. for 24 h. The solvent was removed under reduced pressure to afford 8 g (84%) of a diastereomeric mixture of (1R,E)-N-(2-methylcyclohexylidene)-1-phenylethanamine (I-8a) as a pale yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09447039B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-a6494b17610041718444964d445c6e04 |
| 출처 메모 | uspto-grants-2016_09 |