3,3'-Diaminobenzidine → 4-(2-(4-Methoxyphenyl)-1H-benzo[d]imidazol-6-yl)benzene-1,2-diamine
반응식
[C:1]1([C:9]2[CH:14]=[CH:13][C:12]([NH2:15])=[C:11]([NH2:16])[CH:10]=2)[CH:6]=[CH:5][C:4]([NH2:7])=[C:3]([NH2:8])[CH:2]=1.[CH3:17][O:18][C:19]1[CH:26]=[CH:25][C:22]([CH:23]=O)=[CH:21][CH:20]=1>>[CH3:17][O:18][C:19]1[CH:26]=[CH:25][C:22]([C:23]2[NH:16][C:11]3[CH:10]=[C:9]([C:1]4[CH:2]=[C:3]([NH2:8])[C:4]([NH2:7])=[CH:5][CH:6]=4)[CH:14]=[CH:13][C:12]=3[N:15]=2)=[CH:21][CH:20]=1참가 물질
3
반응 조건
- 온도
- 180 °C
실험 절차
Prepared by Method 2, using a 1:1 ratio of biphenyl-3,3′,4,4′-tetraamine to 4-methoxybenzaldehyde, and heating to 180° C. for 10 min.
후처리
- customPrepared by Method 2
출처 및 근거
- ORD 기록
- ord-53a1bb8bdf2742ab9f0caf12a0b73210
- 출처 데이터셋
- uspto-grants-2016_04
- 특허 번호
- US09314456B2
반응 노트
불러오는 중…