3,3'-Diaminobenzidine → 4-(2-(4-Methoxyphenyl)-1H-benzo[d]imidazol-6-yl)benzene-1,2-diamine

HRID 628580

반응식

HRID 628580 반응식
[C:1]1([C:9]2[CH:14]=[CH:13][C:12]([NH2:15])=[C:11]([NH2:16])[CH:10]=2)[CH:6]=[CH:5][C:4]([NH2:7])=[C:3]([NH2:8])[CH:2]=1.[CH3:17][O:18][C:19]1[CH:26]=[CH:25][C:22]([CH:23]=O)=[CH:21][CH:20]=1>>[CH3:17][O:18][C:19]1[CH:26]=[CH:25][C:22]([C:23]2[NH:16][C:11]3[CH:10]=[C:9]([C:1]4[CH:2]=[C:3]([NH2:8])[C:4]([NH2:7])=[CH:5][CH:6]=4)[CH:14]=[CH:13][C:12]=3[N:15]=2)=[CH:21][CH:20]=1

참가 물질

3

반응물 2

HCID 70713,3'-DiaminobenzidineHCID 312444-Methoxybenzaldehyde

생성물 1

HCID 120309844-(2-(4-Methoxyphenyl)-1H-benzo[d]imidazol-6-yl)benzene-1,2-diamine

반응 조건

온도
180 °C

실험 절차

Prepared by Method 2, using a 1:1 ratio of biphenyl-3,3′,4,4′-tetraamine to 4-methoxybenzaldehyde, and heating to 180° C. for 10 min.

후처리

  1. customPrepared by Method 2

출처 및 근거

ORD 기록
ord-53a1bb8bdf2742ab9f0caf12a0b73210
출처 데이터셋
uspto-grants-2016_04
특허 번호
US09314456B2

연결된 노트

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