2-Propanethiol → HCID 90118331, 화합물

HRID 62868

반응식

HRID 62868 반응식
[CH2:1]([O:3][C:4]([C:6]1[CH:11]=[CH:10][N:9]=[C:8](Cl)[N:7]=1)=[O:5])[CH3:2].[CH3:13][CH:14]([SH:16])[CH3:15]>>[CH2:1]([O:3][C:4]([C:6]1[CH:11]=[CH:10][N:9]=[C:8]([S:16][CH:14]([CH3:15])[CH3:13])[N:7]=1)=[O:5])[CH3:2]

참가 물질

3

반응물 2

HCID 63642-PropanethiolHCID 22509306Ethyl 2-chloropyrimidine-4-carboxylate

생성물 1

HCID 90118331HCID 90118331, 화합물수율 68%

실험 절차

2-Chloropyrimidine-4-carboxylic acid ethyl ester (0.024 g, 0.13 mmol) obtained in Step A and 2-propanethiol were reacted in the same manner as in Step A of Preparation Example 16 to obtain the title compound (0.02 g, 68%).

출처 및 근거

ORD 기록
ord-bb76834c5a184a2880af0b5f4d64a1de
출처 데이터셋
uspto-grants-2016_09
특허 번호
US09447044B2

연결된 노트

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