1,2,3-Trichloropropane → 1,1,2,3-Tetrachloro-1-propene

HRID 631758

반응식

HRID 631758 반응식
ClCC(Cl)CCl.C1C(Cl)=C(Cl)C=C(Cl)C=1OCCO.[Cl:20][CH:21]([Cl:27])[C:22](Cl)([Cl:25])[CH2:23][Cl:24].[Cl:28][C:29]([Cl:35])([Cl:34])[CH:30]([Cl:33])[CH2:31]Cl.ClC(Cl)(Cl)C(Cl)(Cl)C>>[Cl:33][C:30]([C:29]([Cl:35])([Cl:34])[Cl:28])=[CH2:31].[Cl:20][C:21]([Cl:27])=[C:22]([Cl:25])[CH2:23][Cl:24]

참가 물질

7

반응물 5

HCID 72851,2,3-TrichloropropaneHCID 16462FenteracolHCID 855621,1,2,2,3-PentachloropropaneHCID 186684Propane, pentachloro-HCID 134544911,1,1,2,3-Pentachloropropane

생성물 2

HCID 252811,1,2,3-Tetrachloro-1-propeneHCID 5887421-Propene, 2,3,3,3-tetrachloro-

실험 절차

The overhead stream comprising 1,2,3-trichloropropane, TCPE, tetrachloropropanes, 1,1,2,2,3-pentachloropropane, 1,1,1,2,3-pentachloropropane, and 1,1,1,2,2-pentachloropropane is then provided to a reactor where it is dehydrochlorinated to provide dichloropropenes, trichloropropenes, 2,3,3,3-tetrachloropropene, and 1,1,2,3-tetrachloropropene. More specifically, dehydrochlorination reactor may typically be a batch or a continuous stirred tank reactor. The mixing can be done, e.g., by mechanical or jet mixing of feed streams. Those of ordinary skill in the art are readily able to determine the appropriate conditions at which to run a dehydrochlorination reactor in order to conduct the aforementioned dehydrochlorination.

후처리

  1. customis then provided to a reactor where it

출처 및 근거

ORD 기록
ord-3982892dfcc3409083277abf43af557c
출처 데이터셋
uspto-grants-2016_04
특허 번호
US09321707B2

연결된 노트

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