6-Ethylpyridin-2-amine → 6-Ethyl-5-iodopyridin-2-amine

HRID 632879

반응식

HRID 632879 반응식
[CH2:1]([C:3]1[N:8]=[C:7]([NH2:9])[CH:6]=[CH:5][CH:4]=1)[CH3:2].C1C(=O)N([I:17])C(=O)C1>>[CH2:1]([C:3]1[N:8]=[C:7]([NH2:9])[CH:6]=[CH:5][C:4]=1[I:17])[CH3:2]

참가 물질

3

반응물 2

HCID 890216-Ethylpyridin-2-amineHCID 120273N-Iodosuccinimide

생성물 1

HCID 216639766-Ethyl-5-iodopyridin-2-amine

실험 절차

The title compound is synthesized according to general procedure GP1 starting from 10.0 g (83 mmol) 6-ethyl-pyridin-2-ylamine and 18.4 g (83 mmol) NIS. Yield after precipitation from the reaction mixture: 18.0 g (89%).

후처리

  1. customYield
  2. customafter precipitation from the reaction mixture

출처 및 근거

ORD 기록
ord-97088203a1bc4b929148c359aaad85d1
출처 데이터셋
uspto-grants-2016_04
특허 번호
US09321771B2

연결된 노트

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