Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → HCID 15382693, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 4-Nitrobenzoyl chloride | HCID 8502 | — |
| 반응물 | N-benzoyl-2'-deoxyadenosine | HCID 107558 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 15382693 | HCID 15382693 | — |
반응 단계
The synthesis of this product is carried out by reacting 1 eq of p-nitrobenzoyl chloride with 6-N-benzoyldeoxyadenosine for 4 hours in pyridine. After hydrolysis of the excess reagent, partial evaporation of the pyridine, extraction and evaporation of the chloroformic phase, the product is obtained by column chromatography (elution 4% methanol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06187914B1 |
| 출처 데이터셋 | uspto-grants-2001_02 |
| ORD ID | ord-5abaca9d871242a3abe42dc791ab9001 |
| 출처 메모 | uspto-grants-2001_02 |