Water → HCID 178513042, 화합물

반응식

[NH2:1][S:2]([OH:5])(=[O:4])=[O:3].[C:6]([N:8]=[C:9]([NH2:11])[NH2:10])#[N:7].[OH2:12]>>[S:2](=[O:4])(=[O:3])([OH:5])[NH2:1].[C:9]([NH:8][C:6]([NH2:7])=[O:12])(=[NH:11])[NH2:10]

참가 물질

반응물 3

HCID 962Water

HCID 5987Sulfamic Acid

HCID 10005Dicyandiamide

생성물 1

HCID 178513042HCID 178513042, 화합물수율 95%

실험 절차

Sulfaminic acid (97 g) was added batchwise to a solution composed of 84 g dicyandiamide and 300 ml of water at 80° C. whereby the temperature was not permitted to exceed about 95° C. After addition was complete, the temperature was held at 95° C. for 20 minutes, after which the solution was evaporated using a water-jet vacuum. By this process 189 g (=95% of theoretical) guanylurea sulfamate was obtained.