Methyl iodide → HCID 68683485, 화합물

HRID 638928노트

반응식

[CH3:1][O:2][C:3](=[O:16])[C:4]1[CH:9]=[C:8]([O:10][CH3:11])[C:7]([OH:12])=[C:6]([CH2:13][CH:14]=[CH2:15])[CH:5]=1.[CH3:17]I>>[CH3:1][O:2][C:3](=[O:16])[C:4]1[CH:9]=[C:8]([O:10][CH3:11])[C:7]([O:12][CH3:17])=[C:6]([CH2:13][CH:14]=[CH2:15])[CH:5]=1

참가 물질

반응물 2

HCID 6328Methyl iodide

HCID 7131942methyl 3-allyl-4-hydroxy-5-methoxybenzoate

생성물 1

HCID 68683485HCID 68683485, 화합물수율 96%

실험 절차

3-Allyl-4,5-dimethoxybenzoic acid methyl ester was prepared from 3-allyl-4-hydroxy-5-methoxybenzoic acid methyl ester (Example 1, Step 2) by following Method C using methyl iodide as alkylating agent. The reaction was conducted at room temperature for 16 h and crude product was purified by flash column chromatography (96% yield).

후처리

customcrude product was purified by flash column chromatography (96% yield)

출처 및 근거

ORD 기록: ord-ecbe9b079b2447e4a1c9cd9d8e58b046
출처 데이터셋: uspto-grants-2010_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07691843B2

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