Hydroxylamine → 2-Amino-7-ethyl-6,7,8,9-tetrahydro-5H-pyrazino[2,3-d]azepine

HRID 647489노트

반응식

HRID 647489 반응식
Br.[CH2:2]([N:4]1[CH2:10][CH2:9][CH:8](Br)[C:7](=O)[CH2:6][CH2:5]1)[CH3:3].[NH2:13]O.Cl.[NH2:16][CH2:17][C:18]#[N:19]>>[NH2:19][C:18]1[CH:17]=[N:16][C:8]2[CH2:9][CH2:10][N:4]([CH2:2][CH3:3])[CH2:5][CH2:6][C:7]=2[N:13]=1

참가 물질

4

반응물 3

HCID 787HydroxylamineHCID 11491918Aminoacetonitrile hydrochlorideHCID 204364081-Ethyl-5-bromo-hexahydro-azepin-4-one hydrobromide

생성물 1

HCID 30678372-Amino-7-ethyl-6,7,8,9-tetrahydro-5H-pyrazino[2,3-d]azepine

실험 절차

This compound was prepared analogous to Example 40 from 1-ethyl-5-bromo-hexahydro-azepin-4-one hydrobromide, hydroxylamine and α-amino-acetonitrile hydrochloride.

출처 및 근거

ORD 기록
ord-855967ab3aff49b3be4192abfc594a0c
출처 데이터셋
uspto-grants-1983_10
특허 번호
US04409220

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