Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Hydroxide → HCID 14388650, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | p-Toluenesulfonic acid 1-methylheptyl ester | HCID 3912199 | — |
| 반응물 | 4-(4-Acetylphenyl)-2-fluorophenol | HCID 14388649 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 14388650 | HCID 14388650 | 28.6% |
반응 단계
3'-Fluoro-4'-hydroxy-4-acetylbiphenyl (15 g), potassium hydroxide (4.0 g), ethanol (370 ml), optically active 1-methylheptyl p-toluenesulfonate (20.5 g), were heated for 5 hrs. under reflux, to obtain by usual work-up, 6.37 g of 3'-fluoro-4'-(1-methylheptyloxy)-4-acetylbiphenyl, m.p. 67.6°~68.5° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04737313 |
| 출처 데이터셋 | uspto-grants-1988_04 |
| ORD ID | ord-c3224b82c6964637ab80d88d817d7c0d |
| 출처 메모 | uspto-grants-1988_04 |