Ethyl formate → 2-(N-Formyl-2-amino-ethyl)-furan

반응식

[NH2:1][CH2:2][CH2:3][C:4]1[O:5][CH:6]=[CH:7][CH:8]=1.[CH:9](OCC)=[O:10]>>[CH:9]([NH:1][CH2:2][CH2:3][C:4]1[O:5][CH:6]=[CH:7][CH:8]=1)=[O:10]

참가 물질

반응물 2

HCID 8025Ethyl formate

HCID 11328632-(Furan-2-yl)ethan-1-amine

생성물 1

HCID 137469342-(N-Formyl-2-amino-ethyl)-furan

실험 절차

Here, 2-(2-amino-ethyl)furan (10.0 g, 0.090 mol) is refluxed with ethyl formate (80 ml, 1.0 mol) for 12 hours. The reaction product is concentrated by evaporation and distilled in vacuo.

후처리

concentrationThe reaction product is concentrated by evaporation
distillationdistilled in vacuo

출처 및 근거

ORD 기록: ord-c39f5eca83bd43319f039e3f8864241f
출처 데이터셋: uspto-grants-1988_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04737495

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