Methyl iodide → HCID 14555939, 화합물
반응식
[Cl:1][C:2]1[CH:11]=[C:10]2[C:5]([CH:6]=[C:7]([O:12][C:13]3[CH:26]=[CH:25][C:16]([O:17][CH:18]([CH3:24])[C:19]([O:21][CH2:22][CH3:23])=[O:20])=[CH:15][CH:14]=3)[CH:8]=[N:9]2)=[CH:4][CH:3]=1.[CH3:27][I:28]>ClCCl>[I-:28].[Cl:1][C:2]1[CH:11]=[C:10]2[C:5]([CH:6]=[C:7]([O:12][C:13]3[CH:14]=[CH:15][C:16]([O:17][CH:18]([CH3:24])[C:19]([O:21][CH2:22][CH3:23])=[O:20])=[CH:25][CH:26]=3)[CH:8]=[N+:9]2[CH3:27])=[CH:4][CH:3]=1참가 물질
4
실험 절차
Ethyl 2-{4-[(7-chloro-1-methylquinolinium-3-yl)oxy]phenoxy}propionate iodide salt (6) was prepared by reacting a mixture of ethyl 2-{4-[(7-chloroquinolin-3-yl)oxy]phenoxy}propionate (see Example 5) and methyl iodide in dichloromethane at ambient temperature for a period of four days. The product, a viscous oil, was characterized by its proton magnetic resonance spectrum. Pmr spectrum (CDCl3 ; δ in ppm): 9.8 (1H, d); 8.6 (2H, m); 8.3 (1H, d); 7.75 (1H, d of d); 7.1 (4H, d of d); 4.8 (4H, m); 4.15 (2H, q); 1.55 (3H, d); 1.25 (3H, t).