2-Methylpyridine → 2-(2,2-Dichlorovinyl)-benzyl 2-(4-chlorophenyl)-isovalerate

HRID 64919

반응식

HRID 64919 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]([CH:12]([CH3:14])[CH3:13])[C:9](Cl)=[O:10])=[CH:4][CH:3]=1.N1C=CC=CC=1C.[Cl:22][C:23]([Cl:33])=[CH:24][C:25]1[CH:32]=[CH:31][CH:30]=[CH:29][C:26]=1[CH:27]=[O:28]>C1(C)C=CC=CC=1>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]([CH:12]([CH3:14])[CH3:13])[C:9]([O:28][CH2:27][C:26]2[CH:29]=[CH:30][CH:31]=[CH:32][C:25]=2[CH:24]=[C:23]([Cl:22])[Cl:33])=[O:10])=[CH:4][CH:3]=1

참가 물질

5

반응물 3

HCID 79752-MethylpyridineHCID 41780012-(4-Chlorophenyl)-3-methylbutanoyl chlorideHCID 137131312-(2,2-Dichlorovinyl)-benzaldehyde

생성물 1

HCID 137131352-(2,2-Dichlorovinyl)-benzyl 2-(4-chlorophenyl)-isovalerate

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

2.8 g (0.012 mole) of 2-(4-chlorophenyl)-isovaleryl chloride in 50 ml of absolute toluene are introduced into 1.2 g (0.013 mole) of -picoline and 3.2 g (0.015 mole) of 2-(2,2-dichlorovinyl)-benzaldehyde in a conical flask at room temperature, while stirring. After 30 minutes, the mixture is filtered under suction over silica gel, and washing is carried out with toluene.

후처리

  1. filtrationthe mixture is filtered under suction over silica gel
  2. washwashing

출처 및 근거

ORD 기록
ord-0f238b4ef3e5448f8833fd83cb856d4f
출처 데이터셋
uspto-grants-1986_09
특허 번호
US04611010

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