Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Chloro-2-methylbenzoxazole → 5-Chloro-3-(2-methanesulfonylaminoethyl)-2-methylbenzoxazolium 4-chlorobenzenesulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Chloro-2-methylbenzoxazole | HCID 29510 | — |
| 반응물 | 2-Methanesulfonylaminoethyl-4-chlorobenzenesulfonate | HCID 20141389 | — |
| 생성물 | 5-Chloro-3-(2-methanesulfonylaminoethyl)-2-methylbenzoxazolium 4-chlorobenzenesulfonate | HCID 20141390 | — |
반응 단계
The desired crystal was obtained by carrying out the same synthesis as used in Synthesis Example 1 using 4.2 g (25 mmols) of 5-chloro-2-methylbenzoxazole and 15.7 g (50 mmols) of 2-methanesulfonylaminoethyl-4-chlorobenzenesulfonate. Yield: 7.3 g (60.8%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04740455 |
| 출처 데이터셋 | uspto-grants-1988_04 |
| ORD ID | ord-27966be9b7d9455fb4b3588ee65298e9 |
| 출처 메모 | uspto-grants-1988_04 |