HCID 21709913, 화합물 → HCID 21709932, 화합물
반응식
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[N:8]1[C:12](=[O:13])[N:11]=[N:10][NH:9]1.[CH3:14][N:15]([CH:19]1[CH2:24][CH2:23][S:22][CH2:21][CH2:20]1)[C:16](Cl)=[O:17]>CN(C)C1C=CN=CC=1>[CH3:14][N:15]([CH:19]1[CH2:24][CH2:23][S:22][CH2:21][CH2:20]1)[C:16]([N:11]1[C:12](=[O:13])[N:8]([C:3]2[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=2[Br:1])[N:9]=[N:10]1)=[O:17]참가 물질
4
실험 절차
Similarly to the process described in Example 1, 2.5 g (10 mmol) of 1-(2-bromophenyl)-1,2-dihydro-5H-tetrazol-5-one, 2 g (10 mmol) of N-methyl-N-(tetrahydro-2H-thiopyran-4-yl)carbamoyl chloride and 1.5 g (12 mmol) of 4-dimethylaminopyridine were reacted. Yield 2.5 g.
후처리
- customwere reacted
출처 및 근거
- ORD 기록
- ord-7b40b2bb5e034993b8a28ed5d0d229af
- 출처 데이터셋
- uspto-grants-2001_08
- 특허 번호
- US06277790B1
반응 노트
불러오는 중…