Chloride → 4-Methoxy-3-(trifluoromethyl)benzoyl chloride

HRID 650957

반응식

HRID 650957 반응식
[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7](O)=[O:8])=[CH:5][C:4]=1[C:12]([F:15])([F:14])[F:13].[Cl-:16].CN(C=O)C>C(Cl)(Cl)Cl>[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([Cl:16])=[O:8])=[CH:5][C:4]=1[C:12]([F:15])([F:14])[F:13]

참가 물질

5

반응물 3

HCID 312ChlorideHCID 6228DimethylformamideHCID 27752954-Methoxy-3-(trifluoromethyl)benzoic acid

생성물 1

HCID 27752984-Methoxy-3-(trifluoromethyl)benzoyl chloride

시약·촉매·용매 1

HCID 6212Chloroform용매

실험 절차

The title compound was prepared from 4-methoxy-3-trifluoromethylbenzoic acid with oxalkyl chloride and DMF in chloroform at room temperature followed by evaporation in vacua.

후처리

  1. customfollowed by evaporation in vacua

출처 및 근거

ORD 기록
ord-13a5beb60f624fdc98a3a45284514b0a
출처 데이터셋
uspto-grants-2001_08
특허 번호
US06277861B1

연결된 노트

불러오는 중…