Bromine → HCID 22597763, 화합물

HRID 650959노트

반응식

HRID 650959 반응식
[CH3:1][O:2][C:3]1[CH:11]=[C:10]([CH:12]([CH3:14])[CH3:13])[CH:9]=[CH:8][C:4]=1[C:5]([OH:7])=[O:6].[Br:15]Br>C(Cl)(Cl)Cl>[Br:15][C:9]1[C:10]([CH:12]([CH3:14])[CH3:13])=[CH:11][C:3]([O:2][CH3:1])=[C:4]([CH:8]=1)[C:5]([OH:7])=[O:6]

참가 물질

4

반응물 2

HCID 24408BromineHCID 126137372-Methoxy-4-(propan-2-yl)benzoic acid

생성물 1

HCID 22597763HCID 22597763, 화합물

시약·촉매·용매 1

HCID 6212Chloroform용매2회

실험 절차

To a solution of 2-methoxy-4-iso-propyl benzoic acid (7.0 g, 36.0 mmol) in chloroform (100 ml) was added bromine (1.86 ml) in chloroform (20 ml) dropwise. The reaction was stirred at room temperature overnight Evaporation in vacuo afforded an oil (9.27 g). m/z (CI): 275, 273 (MH+; 70%).

후처리

  1. customEvaporation in vacuo

출처 및 근거

ORD 기록
ord-dac6b3c6de964a00a9ea2a0be5deba9f
출처 데이터셋
uspto-grants-2001_08
특허 번호
US06277861B1

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