Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Azaindole → HCID 54447290, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Azaindole | HCID 9220 | — |
| 반응물 | tert-Butyl bromoacetate | HCID 79177 | — |
| 생성물 | HCID 54447290 | HCID 54447290 | — |
반응 단계
The title compound is prepared from 1H-pyrrolo[3,2-c]pyridine as described in EXAMPLES 18 and 19, Part A using tert-butyl bromoacetate in place of methyl iodide. The crude product is purified by column chromatography eluting with a gradient of 3% MeOH/CH2Cl2 to 6% MeOH/CH2Cl2 to give the title compound as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06281227B1 |
| 출처 데이터셋 | uspto-grants-2001_08 |
| ORD ID | ord-b83882fafd474bdaa10245e91d475de6 |
| 출처 메모 | uspto-grants-2001_08 |