Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Peroxide → HCID 13911126, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Peroxide | HCID 784 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 25-Hydroxycholesta-1,4,6-trien-3-one | HCID 22797387 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 13911126 | HCID 13911126 | — |
반응 단계
The trienone from (a) (1.3 gms) in ethanol (50 mls) was treated with 10% aqueous potassium hydroxide (0.5 ml) and 30% aqueous H2O2 (3 ml). After storage overnight at room temperature, the solution was diluted with water and the solid product collected. Recrystallization from aqueous methanol gave the title compound which after one further crystallization had melting point 162°-163°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04670190 |
| 출처 데이터셋 | uspto-grants-1987_06 |
| ORD ID | ord-c0d60886cd6b4abc8e6870ceca398957 |
| 출처 메모 | uspto-grants-1987_06 |