Hydrochloric Acid → Trichloroacetonitrile

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[Cl:1][CH2:2][CH2:3][CH2:4][C:5]1N=[C:9]([C:11]([Cl:14])([Cl:13])[Cl:12])[N:8]=C(C(Cl)(Cl)Cl)[N:6]=1.Cl>>[Cl:12][C:11]([Cl:14])([Cl:13])[C:9]#[N:8].[Cl:1][CH2:2][CH2:3][CH2:4][C:5]#[N:6]

참가 물질

반응물 2

HCID 313Hydrochloric Acid

HCID 201996122-(gamma-Chloropropyl)4,6-bis-(trichloromethyl)-1,3,5-triazine

생성물 2

HCID 11011Trichloroacetonitrile

HCID 123364-Chlorobutyronitrile

실험 절차

The 2-amino-4-cyclopropyl-triazines of formula I can also be prepared, starting from a 2-(γ-chloropropyl)4,6-bis-(trichloromethyl)-1,3,5-triazine, which is obtained by condensation of 2 moles of trichloroacetonitrile and one mol of γ-chlorobutyronitrile in the presence of hydrogen chloride. ##STR6##

출처 및 근거

ORD 기록: ord-c2d5effca1b4435884a019d45a0ffdb0
출처 데이터셋: uspto-grants-1987_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04670559

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