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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 652803생성일: 2026년 10월 25일

3-Benzyloxy-4-methoxybenzaldehyde → 2-Chloro-3-benzyloxy-4-hydroxybenzaldehyde

https://huagongshe.com/reaction/652803

반응식

참여 물질

역할이름HCID투입량
반응물3-Benzyloxy-4-methoxybenzaldehydeHCID 80671—
반응물2-Chloro-3-benzyloxy-4-methoxybenzaldehydeHCID 11747833—
생성물2-Chloro-3-benzyloxy-4-hydroxybenzaldehydeHCID 20196371—

반응 단계

Proceeding as in example 62, but replacing for 3-benzyloxy-4-methoxybenzaldehyde an equivalent quantity of 2-chloro-3-benzyloxy-4-methoxybenzaldehyde (obtained as described in example 84) and purifying the reaction raw product by chromatography on a silica gel column, eluting with methylene chloride/petroleum ether (b.p. 30°-70° C.)=1/1, 2-chloro-3-benzyloxy-4-hydroxybenzaldehyde was obtained, m.p. 149°-150° C. (from methylene chloride/petrolum ether, b.p. 30°-70° C.=1/2).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04673671
출처 데이터셋uspto-grants-1987_06
ORD IDord-739ed3bb4d6e463d979b86957dd70310
출처 메모uspto-grants-1987_06