Pyrrolidine → HCID 13531608, 화합물

HRID 653093노트

반응식

HRID 653093 반응식
Br[CH2:2][C:3]1[CH:4]=[CH:5][C:6]2[O:10][C:9]([N+:11]([O-:13])=[O:12])=[C:8]([C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[C:7]=2[CH:20]=1.[NH:21]1[CH2:25][CH2:24][CH2:23][CH2:22]1>C(O)C>[N+:11]([C:9]1[O:10][C:6]2[CH:5]=[CH:4][C:3]([CH2:2][N:21]3[CH2:25][CH2:24][CH2:23][CH2:22]3)=[CH:20][C:7]=2[C:8]=1[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)([O-:13])=[O:12]

참가 물질

4

반응물 2

HCID 31268PyrrolidineHCID 13531604HCID 13531604, 화합물

생성물 1

HCID 13531608HCID 13531608, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

Using the method of Example 1, 5-bromomethyl-2-nitro-3-phenylbenzofuran is reacted with pyrrolidine in ethanol to provide yellow crystals of 2-nitro-3-phenyl-5-(1-pyrrolidylmethyl)benzofuran, m.p. 111°-112.5° C., having the structure

출처 및 근거

ORD 기록
ord-ec441d43808a47a58c84b03ec99db0dc
출처 데이터셋
uspto-grants-1987_06
특허 번호
US04675320

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