Methyl iodide → HCID 13531615, 화합물

HRID 653098노트

반응식

HRID 653098 반응식
[N+:1]([C:4]1[O:5][C:6]2[CH:18]=[CH:17][C:16]([CH2:19][N:20]3[CH2:24][CH2:23][CH2:22][CH2:21]3)=[CH:15][C:7]=2[C:8]=1[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)([O-:3])=[O:2].[CH3:25][I:26]>CC(C)=O>[I-:26].[CH3:25][N+:20]1([CH2:19][C:16]2[CH:17]=[CH:18][C:6]3[O:5][C:4]([N+:1]([O-:3])=[O:2])=[C:8]([C:9]4[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=4)[C:7]=3[CH:15]=2)[CH2:24][CH2:23][CH2:22][CH2:21]1

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 13531608HCID 13531608, 화합물2회

생성물 1

HCID 13531615HCID 13531615, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

Using the method of Example 8, 2-nitro-3-phenyl-5-(1-pyrrolidylmethyl)benzofuran (the product of Example 2) is reacted with methyliodide in acetone to provide tan solid N-methyl-N-(2-nitro-3-phenyl-5-benzofuranylmethyl)pyrrolidinium iodide, m.p. 235°-237° C., having the structure

출처 및 근거

ORD 기록
ord-43f94027058e4c7e86a4c30870e0b034
출처 데이터셋
uspto-grants-1987_06
특허 번호
US04675320

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