Sodium Hydroxide → Sodium 2-chloro-3-benzyloxypropionate
반응식
[Cl:1][CH:2]([CH2:6][O:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)[C:3]([OH:5])=[O:4].[OH-].[Na+:16]>O>[Cl:1][CH:2]([CH2:6][O:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)[C:3]([O-:5])=[O:4].[Na+:16]참가 물질
4
실험 절차
85 g of 2-chloro-3-benzyloxypropionic acid (0.396 mol) were suspended in 550 ml of water and neutralized to pH 7 with 10% sodium hydroxide. After stirring for 15 min, the resulting aqueous solution was washed with ethyl ether and evaporated to dryness under vacuum to give the desired compound.
후처리
- washthe resulting aqueous solution was washed with ethyl ether
- customevaporated to dryness under vacuum
출처 및 근거
- ORD 기록
- ord-ce6d7bc3a6f446ad8c73792b287efab1
- 출처 데이터셋
- uspto-grants-1992_07
- 특허 번호
- US05132409
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