N-Methylacetamide → methylvinyldi-(N-methylacetamido)silane
반응식
[Na].[CH3:2][NH:3][C:4](=[O:6])[CH3:5].[CH3:7][CH:8]=[CH:9][SiH:10](Cl)Cl>C1(C)C=CC=CC=1>[CH3:7][CH:8]=[CH:9][SiH:10]([N:3]([CH3:2])[C:4](=[O:6])[CH3:5])[N:3]([CH3:2])[C:4](=[O:6])[CH3:5]참가 물질
5
실험 절차
An illustration of the method for preparing the amidosilanes is as follows: mixing a sodium salt of N-methylacetamide with methylvinyldichlorosilane in an inert organic solvent such as toluene, filtering the by-produced sodium chloride from the toluene-product solution and thereafter removing the toluene by vacuum distillation to obtain the product, methylvinyldi-(N-methylacetamido)silane.
후처리
- filtrationfiltering the by-produced sodium chloride from the toluene-product solution
- customremoving the toluene
- distillationby vacuum distillation
출처 및 근거
- ORD 기록
- ord-22102bcdd36045b4b1cb1f0914de7253
- 출처 데이터셋
- uspto-grants-1986_09
- 특허 번호
- US04614760
반응 노트
불러오는 중…