Diethylmethylamine → Methanesulfonic acid, 1,1,1-trifluoro-, compd. with N-ethyl-N-methylethanamine (1:1)

HRID 655087

반응식

HRID 655087 반응식
[CH2:1]([N:3]([CH2:5][CH3:6])[CH3:4])[CH3:2].[F:7][C:8]([F:14])([F:13])[S:9]([OH:12])(=[O:11])=[O:10]>>[F:7][C:8]([F:14])([F:13])[S:9]([O-:12])(=[O:11])=[O:10].[CH2:1]([NH+:3]([CH2:5][CH3:6])[CH3:4])[CH3:2]

참가 물질

3

반응물 2

HCID 12022Diethylmethylamine2회HCID 62406Trifluoromethanesulfonic acid2회

생성물 1

HCID 86620365Methanesulfonic acid, 1,1,1-trifluoro-, compd. with N-ethyl-N-methylethanamine (1:1)

실험 절차

Equimolar amounts of diethylmethylamine and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed diethylmethylamine and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

후처리

  1. temperaturewhile being cooled by liquid nitrogen
  2. customthus obtaining a target ionic conductor

출처 및 근거

ORD 기록
ord-9f5289c08f2941199dbef871e4dcb7eb
출처 데이터셋
uspto-grants-2011_12
특허 번호
US08071253B2

연결된 노트

불러오는 중…