Trifluoromethanesulfonic acid → Ethylpiperidinium Trifluoromethanesulfonate

반응식

[CH2:1]([NH+:3]1[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1)[CH3:2].[F:9][C:10]([F:16])([F:15])[S:11]([OH:14])(=[O:13])=[O:12]>>[F:9][C:10]([F:16])([F:15])[S:11]([O-:14])(=[O:13])=[O:12].[CH2:1]([NH+:3]1[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1)[CH3:2]

참가 물질

반응물 2

HCID 62406Trifluoromethanesulfonic acid2회

HCID 6992606HCID 6992606, 화합물2회

생성물 1

HCID 23134843Ethylpiperidinium Trifluoromethanesulfonate

실험 절차

Equimolar amounts of ethylpiperidinium and trifluoromethanesulfonic acid were weighed in a glove box under argon atmosphere. The weighed ethylpiperidinium and trifluoromethanesulfonic acid were mixed and stirred while being cooled by liquid nitrogen, thus obtaining a target ionic conductor.

후처리

temperaturewhile being cooled by liquid nitrogen
customthus obtaining a target ionic conductor

출처 및 근거

ORD 기록: ord-992faf3e5286475382865b9ae13d094b
출처 데이터셋: uspto-grants-2011_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08071253B2

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