Hydrochloric Acid → Benzenediazonium chloride

HRID 65551

반응식

HRID 65551 반응식
[ClH:1].[NH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.Cl.[N:10]([O-])=O.[Na+]>O>[Cl-:1].[C:3]1([N+:2]#[N:10])[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 8870Benzenamine hydrochloride (1:1)HCID 23668193Sodium Nitrite

생성물 1

HCID 60992Benzenediazonium chloride

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

A solution of benzenediazonium chloride was prepared as follows: To an ice cold (about 5° C.) solution of aniline hydrochloride (3.24 g., 25 mmoles) in water (10 ml.) and concentrated hydrochloric acid (2.1 ml., 25 mmoles) was added dropwise with stirring a solution of sodium nitrite (1.9 g., 27.5 mmoles) in water (10 ml.). After addition the solution was stirred in the cold for an additional 15 minutes.

후처리

  1. additionAfter addition the solution

출처 및 근거

ORD 기록
ord-9a32150a3bf545fe94a430c25ee8ca32
출처 데이터셋
uspto-grants-1978_12
특허 번호
US04128425

연결된 노트

불러오는 중…