Methyl 3-(2,3-dichlorophenyl)propionate → 3-(2,3-Dichlorophenyl)propanoic acid

HRID 65732노트

반응식

HRID 65732 반응식
[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:9][CH2:10][C:11]([O:13]C)=[O:12]>[OH-].[Na+]>[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:9][CH2:10][C:11]([OH:13])=[O:12]

참가 물질

3

반응물 1

HCID 12595092Methyl 3-(2,3-dichlorophenyl)propionate

생성물 1

HCID 125951013-(2,3-Dichlorophenyl)propanoic acid

시약·촉매·용매 1

HCID 14798Sodium Hydroxide용매

실험 절차

Methyl 3-(2,3-dichlorophenyl)propionate was refluxed in 10% aqueous sodium hydroxide (1 l.) for two hours and the reaction mixture was cooled, acidified and filtered. The filter cake was dissolved in hot aqueous sodium bicarbonate, and filtered. The filtrate was acidified and filtered to yield 3-(2,3-dichlorophenyl)propionic acid.

후처리

  1. temperaturethe reaction mixture was cooled
  2. filtrationfiltered
  3. dissolutionThe filter cake was dissolved in hot aqueous sodium bicarbonate
  4. filtrationfiltered
  5. filtrationfiltered

출처 및 근거

ORD 기록
ord-000a1bced82f4a62a15526285accafb3
출처 데이터셋
uspto-grants-1978_12
특허 번호
US04128666

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