Ethanol → Sodium 8-aminonaphthalene-1,3,5-trisulfonate

HRID 65901

반응식

HRID 65901 반응식
[NH2:1][C:2]1[C:11]2[C:10]([S:12]([OH:15])(=[O:14])=[O:13])=[CH:9][C:8]([S:16]([OH:19])(=[O:18])=[O:17])=[CH:7][C:6]=2[C:5]([S:20]([OH:23])(=[O:22])=[O:21])=[CH:4][CH:3]=1.[OH-].[Na+:25].C(O)C>O>[Na+:25].[Na+:25].[Na+:25].[NH2:1][C:2]1[C:11]2[C:10]([S:12]([O-:15])(=[O:14])=[O:13])=[CH:9][C:8]([S:16]([O-:19])(=[O:17])=[O:18])=[CH:7][C:6]=2[C:5]([S:20]([O-:23])(=[O:22])=[O:21])=[CH:4][CH:3]=1

참가 물질

5

반응물 3

HCID 702EthanolHCID 14798Sodium HydroxideHCID 873558-Aminonaphthalene-1,3,5-trisulfonic acid

생성물 1

HCID 10343683Sodium 8-aminonaphthalene-1,3,5-trisulfonate

시약·촉매·용매 1

HCID 962Water용매

실험 절차

To a mixture of 26.6 g of 8-amino-1,3,5-naphthalenetrisulfonic acid in 25 ml of water is added 12 ml of 5N sodium hydroxide. This solution is added to 125 ml of ethanol and stirred for 30 minutes. The resulting solid is recovered by filtration, washed with 50 ml of 80% ethanol followed by ethanol and ether and dried at 110° C. giving 8-amino-1,3,5-naphthalenetrisulfonic acid trisodium salt.

후처리

  1. filtrationThe resulting solid is recovered by filtration
  2. washwashed with 50 ml of 80% ethanol
  3. customdried at 110° C.

출처 및 근거

ORD 기록
ord-63dad3697ee74cb4b39486bd094061c4
출처 데이터셋
uspto-grants-1978_12
특허 번호
US04129591

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