Methyl iodide → 2-Ethyl-4,6-bis-trifluoromethyl-benzoic acid

HRID 659218

반응식

HRID 659218 반응식
CO[C:3]1C=C(C(F)(F)F)C=C(SC)[C:4]=1C(O)=O.[F:18][C:19]([F:34])([F:33])[C:20]1[CH:28]=[C:27]([C:29]([F:32])([F:31])[F:30])[CH:26]=[CH:25][C:21]=1[C:22]([OH:24])=[O:23].IC>>[CH2:3]([C:25]1[CH:26]=[C:27]([C:29]([F:32])([F:30])[F:31])[CH:28]=[C:20]([C:19]([F:33])([F:34])[F:18])[C:21]=1[C:22]([OH:24])=[O:23])[CH3:4]

참가 물질

4

반응물 3

HCID 6328Methyl iodideHCID 1417522,4-Bis(trifluoromethyl)benzoic acidHCID 591979212-Methoxy-6-methylsulfanyl-4-trifluoromethyl-benzoic acid

생성물 1

HCID 591979342-Ethyl-4,6-bis-trifluoromethyl-benzoic acid

실험 절차

The title compound, white solid, MS: m/e=285.2 [(M−H)−], was prepared in accordance with the general method of intermediate A from 2,4-bis(trifluoromethyl)benzoic acid and iodomethane.

출처 및 근거

ORD 기록
ord-fd09ffd52b93448684ea4e01ef993865
출처 데이터셋
uspto-grants-2011_12
특허 번호
US08080541B2

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