Phosphorus oxychloride → Imidazo[1,5-a]quinoline

HRID 66024노트

반응식

HRID 66024 반응식
[CH:1]([NH:3][CH2:4][C:5]1[CH:14]=[CH:13][C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[N:6]=1)=O.P(Cl)(Cl)(Cl)=O>>[CH:1]1[N:6]2[C:7]3[C:12]([CH:13]=[CH:14][C:5]2=[CH:4][N:3]=1)=[CH:11][CH:10]=[CH:9][CH:8]=3

참가 물질

3

반응물 2

HCID 24813Phosphorus oxychlorideHCID 118301332-Quinolinylmethylformamide

생성물 1

HCID 11073814Imidazo[1,5-a]quinoline

실험 절차

Treatment of 1.86 g. of 2-formamidomethylquinoline with 15 ml. of phosphorous oxychloride as in Preparation AIII-a gave imidazo[1,5-a]quinoline, which is used without purification.

출처 및 근거

ORD 기록
ord-18aa7721ed8a4191a0189f0643e52684
출처 데이터셋
uspto-grants-1978_12
특허 번호
US04129567

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