Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylformamide dimethyl acetal → Hexahydro-2a1H-2a,4a,6a-triazacyclopenta[cd]pentalene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 반응물 | 1,4,7-Triazacyclononane | HCID 188318 | — |
| 생성물 | Hexahydro-2a1H-2a,4a,6a-triazacyclopenta[cd]pentalene | HCID 10986308 | — |
반응 단계
In a manner similar to that of Example 1 (C), 4.55 g (35.5 mmol) of 1,4,7-triazacyclononane and 4.20 g of dimethylformamide dimethyl acetal were reacted to give 4.33 g (88%) clear, colorless liquid, bp 79°-80° (2.6mm).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04130715 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-64791c2b857b46bbad90fb33b83063ec |
| 출처 메모 | uspto-grants-1978_12 |