Boron trifluoride → Ethylene

HRID 66696

반응식

HRID 66696 반응식
[B:1]([F:4])([F:3])[F:2].CO.[C:7]([O:12][CH3:13])(=[O:11])[CH:8](C)[CH3:9].B(F)(F)F>>[C:7]([O:12][CH3:13])(=[O:11])[CH2:8][CH3:9].[CH2:7]=[CH2:8].[B:1]([F:4])([F:3])[F:2]

참가 물질

5

반응물 2

HCID 6356Boron trifluoride2회HCID 88663997BF3 methanol methyl isobutyrate

생성물 3

HCID 6325EthyleneHCID 6356Boron trifluorideHCID 11124Methyl propionate

실험 절차

In still another approach, an admixture of BF3 /methanol/methyl isobutyrate in a molar ratio of 1:1:0.5 was introduced to the top of a countercurrent stripping column while nitrogen was passed through the bottom of the column under atmospheric pressure at a temperature of 80° C. The effort to preferentially strip the BF3 was unsuccessful. Analysis showed that no BF3 was removed by this technique. Methyl propionate is produced from ethylene and BF3.CH3OH.

후처리

  1. customat a temperature of 80° C
  2. customwas removed by this technique

출처 및 근거

ORD 기록
ord-1e111c1e7f234f0e83ad390347bfb66e
출처 데이터셋
uspto-grants-1982_08
특허 번호
USRE031010

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