4-Methylbenzenethiol → 2-[(4-Methylphenyl)thio]acetonitrile

HRID 66767노트

반응식

HRID 66767 반응식
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([SH:8])=[CH:4][CH:3]=1.Cl[CH2:10][C:11]#[N:12].C([O-])([O-])=O.[K+].[K+]>CS(C)=O>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][CH2:10][C:11]#[N:12])=[CH:4][CH:3]=1

참가 물질

5

반응물 3

HCID 78114-MethylbenzenethiolHCID 7856ChloroacetonitrileHCID 11430Potassium Carbonate

생성물 1

HCID 27997712-[(4-Methylphenyl)thio]acetonitrile

시약·촉매·용매 1

HCID 679Dimethyl Sulfoxide용매

실험 절차

The compound 4-methylthiophenoxyacetonitrile was prepared by heating 4-methylthiophenol, chloroacetonitrile and anhydrous K2CO3 in DMSO, employing substantially the same procedure described in previous examples.

출처 및 근거

ORD 기록
ord-135cec88a4434915a548520ac93a9dd3
출처 데이터셋
uspto-grants-1982_08
특허 번호
US04343808

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