Diazomethane → HCID 20528716, 화합물

HRID 67175노트

반응식

HRID 67175 반응식
[C:1]([C:4]1[CH:14]=[CH:13][CH:12]=[C:6]2[C:7]([NH:9][C:10](=[O:11])[C:5]=12)=[O:8])([OH:3])=[O:2].[N+](=[CH2:17])=[N-]>CCOCC>[CH3:17][O:2][C:1]([C:4]1[CH:14]=[CH:13][CH:12]=[C:6]2[C:7]([NH:9][C:10](=[O:11])[C:5]=12)=[O:8])=[O:3]

참가 물질

4

반응물 2

HCID 9550DiazomethaneHCID 205447191,3-dioxo-2,3-dihydro-1H-isoindole-4-carboxylic acid

생성물 1

HCID 20528716HCID 20528716, 화합물

시약·촉매·용매 1

HCID 3283Diethyl Ether용매2회

실험 절차

To a suspension of 3-carboxyphthalimide (10 g) in ether (50 ml), a solution of diazomethane in ether was added slowly until a faint yellow colouration persisted. Excess of diazomethane was destroyed with acetic acid and the reaction mixture was evaporated to yield the desired compound.

후처리

  1. customExcess of diazomethane was destroyed with acetic acid
  2. customthe reaction mixture was evaporated

출처 및 근거

ORD 기록
ord-76be70ed1a3f490eb78799c7bb42183a
출처 데이터셋
uspto-grants-1982_08
특허 번호
US04345071

반응 노트

불러오는 중…