Bromine → 2-Bromophenacyl Bromide

HRID 6776

반응식

HRID 6776 반응식
[Br:1]Br.[Br:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[C:10](=[O:12])[CH3:11]>C(O)(=O)C>[Br:1][CH2:11][C:10]([C:5]1[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=1[Br:3])=[O:12]

참가 물질

4

반응물 2

HCID 24408BromineHCID 750602'-Bromoacetophenone

생성물 1

HCID 27375222-Bromophenacyl Bromide

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

Bromine (40.3 g, 0.25 mol) was added dropwise to a solution of 2′-Bromoacetophenone (50.0 g, 0.25 mol) in acetic acid (50 ml) over 1.5 hours at 15–20° C. The solution was then allowed to warm to room temperature and concentrated under reduced pressure to yield a crude product that was used without further purification.

후처리

  1. concentrationconcentrated under reduced pressure

출처 및 근거

ORD 기록
ord-eba8a3d7c9cc40e19409ef56651f619b
출처 데이터셋
uspto-grants-2006_08
특허 번호
US07084135B1

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