HCID 13548560, 화합물 → HCID 13548562, 화합물

HRID 703448노트

반응식

HRID 703448 반응식
[O:1]=[C:2]1[CH:11]=[C:10]([CH2:12][C:13](OC)=[O:14])[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[NH:3]1>[Pt]>[OH:14][CH2:13][CH2:12][C:10]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[NH:3][C:2](=[O:1])[CH:11]=1.[OH:14][CH2:13][CH2:12][CH:10]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[NH:3][C:2](=[O:1])[CH2:11]1

참가 물질

4

반응물 1

HCID 13548560HCID 13548560, 화합물

생성물 2

HCID 13548562HCID 13548562, 화합물HCID 14624972(+/-)-4-(2-hydroxyethyl)-3,4-dihydro-2(1H)-quinolinone

시약·촉매·용매 1

HCID 23939Platinum촉매

실험 절차

4-(2-Hydroxyethyl)-2(1H)-quinolinone is prepared from methyl 2-oxo-1,2-dihydro-4-quinolineacetate (prepared in 3.3.) according to the procedure described in 1.3. It is a solid, melting point 213°-5° C. A catalytic hydrogenation of this compound is performed with Adams+ platinum to obtain (±)-4-(2-hydroxyethyl)-3,4-dihydro-2(1H)-quinolinone.

출처 및 근거

ORD 기록
ord-4435f4f9499146569e8f85a164d6c4c5
출처 데이터셋
uspto-grants-1991_01
특허 번호
US04983607

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