Cyanuric chloride → 1,3,5-Triazine, 2,4,6-tris(1-azetidinyl)-

HRID 704114노트

반응식

HRID 704114 반응식
[NH:1]1[CH2:4][CH2:3][CH2:2]1.[N:5]1[C:12](Cl)=[N:11][C:9](Cl)=[N:8][C:6]=1Cl>O>[N:1]1([C:6]2[N:8]=[C:9]([N:1]3[CH2:4][CH2:3][CH2:2]3)[N:11]=[C:12]([N:1]3[CH2:4][CH2:3][CH2:2]3)[N:5]=2)[CH2:4][CH2:3][CH2:2]1

참가 물질

4

반응물 2

HCID 7954Cyanuric chlorideHCID 10422Azetidine

생성물 1

HCID 1520761,3,5-Triazine, 2,4,6-tris(1-azetidinyl)-수율 78%

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Compound LXXVI was prepared after the method of Schaefer (J Am Chem Soc (1955) 77 p592B). The hydrochloride salt of azetidine was reacted with cyanuric chloride in water to give compound LXXVI as a white solid (yield 78%) having a melting point of 225°-238° C. The 1Hnmr of this compound indicated that its identity was correct and that its purity was adequate for subsequent reactions without further purification.

후처리

  1. customCompound LXXVI was prepared after the method of Schaefer (J Am Chem Soc (1955) 77 p592B)

출처 및 근거

ORD 기록
ord-5e35f850284549238e6e160ccc3f5f5b
출처 데이터셋
uspto-grants-1991_01
특허 번호
US04985584

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