Water → HCID 15729558, 화합물
반응식
F[C:2]1[N:7]=[C:6]([S:8](Cl)(=[O:10])=[O:9])[CH:5]=[CH:4][CH:3]=1.Cl.[O:13](N)[CH3:14].C([N:18]([CH2:21]C)CC)C.[OH2:23]>C(Cl)(Cl)Cl>[CH3:14][O:13][N:18]([CH3:21])[S:8]([C:6]1[CH:5]=[CH:4][CH:3]=[C:2]([O:23][S:8]([CH3:6])(=[O:10])=[O:9])[N:7]=1)(=[O:10])=[O:9]참가 물질
6
실험 절차
A solution of 6-fluoropyridine-2-sulphonylchloride (1.96 g) and methoxylamine hydrochloride (1.96 g) in chloroform (40 cm3) was cooled to -78° C. under an atmosphere of nitrogen and a solution of triethylamine (2.03 g) in chloroform (10 cm3) was added with stirring. The reaction mixture was added to water and the product extracted into chloroform. The combined organic layers were dried over magnesium sulphate, filtered and evaporated to give the title product.
후처리
- extractionthe product extracted into chloroform
- dry with materialThe combined organic layers were dried over magnesium sulphate
- filtrationfiltered
- customevaporated
출처 및 근거
- ORD 기록
- ord-ac0c0438638f4a129843754e9c188ddc
- 출처 데이터셋
- uspto-grants-1991_01
- 특허 번호
- US04987141
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