(2-Methoxypyridin-4-yl)methanamine → 4-(Aminomethyl)pyridin-2(1H)-one

HRID 711263

반응식

HRID 711263 반응식
C[O:2][C:3]1[CH:8]=[C:7]([CH2:9][NH2:10])[CH:6]=[CH:5][N:4]=1>Cl>[NH2:10][CH2:9][C:7]1[CH:6]=[CH:5][NH:4][C:3](=[O:2])[CH:8]=1

참가 물질

3

반응물 1

HCID 16227983(2-Methoxypyridin-4-yl)methanamine

생성물 1

HCID 150793014-(Aminomethyl)pyridin-2(1H)-one

시약·촉매·용매 1

HCID 313Hydrochloric Acid용매

실험 절차

The starting material (2-methoxypyridin-4-yl)methanamine 56-2 in 3N HCl was refluxed at 110° C. for 12 hours. The reaction was taken to dryness by rotary evaporation to give crude 4-(aminomethyl)pyridin-2(1H)-one 56-3.

후처리

  1. customThe reaction was taken to dryness by rotary evaporation

출처 및 근거

ORD 기록
ord-0a0113fcf18d4c1b932891df2d2f6d59
출처 데이터셋
uspto-grants-2015_11
특허 번호
US09181235B2

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