Methacrylic Acid → Solanone

HRID 716607노트

반응식

HRID 716607 반응식
C(O)(=O)C(C)=C.CC(C(OCCOC(C(C)=C)=O)=O)=C.[CH:21]([CH:24]([CH2:30][CH2:31][CH:32]([CH3:34])[CH3:33])[CH2:25][CH2:26][C:27](=[O:29])[CH3:28])([CH3:23])[CH3:22]>C1(C)C=CC=CC=1>[CH3:23][CH:21]([C@@H:24](/[CH:30]=[CH:31]/[C:32]([CH3:34])=[CH2:33])[CH2:25][CH2:26][C:27]([CH3:28])=[O:29])[CH3:22]

참가 물질

5

반응물 3

HCID 4093Methacrylic AcidHCID 7355Ethylene glycol dimethacrylateHCID 89183541HCID 89183541, 화합물

생성물 1

HCID 6451337Solanone

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

Methacrylic acid (3 mol percent), EGDMA (95 mol percent), and 5-isopropyl-8-methylnonan-2-one (2 mol percent) are combined in toluene. 2,2-Azobisisobutyronitrile (AIBN) is added as an initiator. The reaction flask is degassed, purged with dry nitrogen, and sealed. The solution is irradiated with a UV lamp (365 nm) to activate the AIBN and initiate the polymerization reaction.

후처리

  1. customThe reaction flask is degassed
  2. custompurged with dry nitrogen
  3. customsealed
  4. customThe solution is irradiated with a UV lamp (365 nm)
  5. customthe polymerization reaction

출처 및 근거

ORD 기록
ord-b5ac5cf49dcf4455a1dc12b61b82caa9
출처 데이터셋
uspto-grants-2015_11
특허 번호
US09192193B2

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