Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethoxysilane → (3-(Methoxymethoxy)-2-methylpropyl)triethoxysilane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethoxysilane | HCID 13830 | — |
| 반응물 | 3-Methoxymethoxy-2-methyl-1-propene | HCID 13694620 | — |
| 촉매 | Platinate(2-), hexachloro-, hydrogen, hydrate (1:2:1), (OC-6-11)- | HCID 16211507 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | (3-(Methoxymethoxy)-2-methylpropyl)triethoxysilane | HCID 86690070 | 39.9% |
반응 단계
Into a 200-ml flask, 5.81 g (50% by mol) of 2-methyl-4,6-dioxa-1-heptene, 0.026 g (0.05% by mol) of hexachloroplatinic(IV) acid hydrate, and 100 g of tetrahydrofuran were charged. Into the mixed solution, 10.68 g (65% by mol) of triethoxysilane was added dropwise under a nitrogen stream with stirring with a magnetic stirrer. After the addition, the mixture was reacted at ambient temperature for 24 hours. Then, the reaction mixture was distilled to afford 5.60 g of (3-(methoxymethoxy)-2-methylpropyl)triethoxysilane (corresponding to the compound of Formula (A-23)).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09196484B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-e21cb9aa4235463fae774f3bfbac3e02 |
| 출처 메모 | uspto-grants-2015_11 |