反应详情

Into a 200-ml flask, 5.81 g (50% by mol) of 2-methyl-4,6-dioxa-1-heptene, 0.026 g (0.05% by mol) of hexachloroplatinic(IV) acid hydrate, and 100 g of tetrahydrofuran were charged. Into the mixed solution, 10.68 g (65% by mol) of triethoxysilane was added dropwise under a nitrogen stream with stirring with a magnetic stirrer. After the addition, the mixture was reacted at ambient temperature for 24 hours. Then, the reaction mixture was distilled to afford 5.60 g of (3-(methoxymethoxy)-2-methylpropyl)triethoxysilane (corresponding to the compound of Formula (A-23)).

1. additionAfter the addition
2. customthe mixture was reacted at ambient temperature for 24 hours
3. distillationThen, the reaction mixture was distilled