Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(3-Chloro-2-thienyl)-1,3-thiazol-2-amine → 2,4-Dichloro-N-[4-(3-chloro-2-thienyl)1,3-thiazol-2-yl]-6-methylbenzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(3-Chloro-2-thienyl)-1,3-thiazol-2-amine | HCID 1488441 | — |
| 반응물 | 2,4-Dichloro-6-methylbenzenesulfonyl chloride | HCID 2801387 | — |
| 생성물 | 2,4-Dichloro-N-[4-(3-chloro-2-thienyl)1,3-thiazol-2-yl]-6-methylbenzenesulfonamide | HCID 10274951 | — |
반응 단계
The title compound was prepared from 4-(3-chloro-2-thienyl)-1,3-thiazol-2-amine and 2,4-dichloro-6-methylbenzenesulfonyl chloride as described in the synthetic METHOD B to give a yellow solid (9.4 mg) with purity >90%: MS (pos) m/z 439.1, 441.1; HRS m/z 437.8875 (calc. of monoisotopic mass for C14H9Cl3N2O2S3 gives 437.8892).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07132436B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-146beaaec28f47d2b1d038b40ab60e58 |
| 출처 메모 | uspto-grants-2006_11 |