Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → 2-Pyridinemethanol, 2-acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 2-Methylpyridine 1-oxide | HCID 13602 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 2-Pyridinemethanol, 2-acetate | HCID 13881 | — |
반응 단계
A solution of the 2-methyl pyridine N-oxide (1.0 mmol) in acetic anhydride (5 mmol) was heated to reflux for 0.5 h. Work-up (EtOAc), drying (MgSO4), evaporation and purification by preparative TLC or flash chromatography afforded the 2-(acetoxymethyl)pyridine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07138401B2 |
| 출처 데이터셋 | uspto-grants-2006_11 |
| ORD ID | ord-46b932fbdc8540ac87584522c6800eb6 |
| 출처 메모 | uspto-grants-2006_11 |