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Chlorotrimethylsilane → HCID 19705234, 화합물

HRID 727181
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HRID 727181 반응식
[Cl:1][C:2]1[CH:3]=[C:4]([C:8](O)([CH3:10])[CH3:9])[CH:5]=[CH:6][CH:7]=1.[Br-:12].[Li+].C[Si](Cl)(C)C>C(#N)C>[Br:12][C:8]([C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([Cl:1])[CH:3]=1)([CH3:10])[CH3:9]
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참가 물질

5

반응물 3

HCID 6397ChlorotrimethylsilaneHCID 82050Lithium BromideHCID 593110Benzenemethanol, 3-chloro-alpha,alpha-dimethyl-

생성물 1

HCID 19705234HCID 19705234, 화합물

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

This compound is prepared in a manner analogous to that of Step A of Example 5, using 8.5 grams (0.05 mole) of 2-(3-chlorophenyl)propan-2-ol, 8.7 grams (0.1 mole) of lithium bromide, and 13.5 grams (0.125 mole) of trimethylsilyl chloride in 100 mL of acetonitrile, yielding 2-bromo-2-(3-chlorophenyl)propane.

후처리

  1. customThis compound is prepared in a manner analogous to that of Step A of Example 5

출처 및 근거

ORD 기록
ord-b54c55974a5c42bb8a03d7cd5eecabf8
출처 데이터셋
uspto-grants-1998_01
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US05712281

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